T10-11 Homogenous Detection of Fumonisin B1 with Molecule Beacon Based on Fluorescence Resonance Energy Transfer between Upconversion Nanoparticles and Gold Nanoparticles

Wednesday, July 25, 2012: 11:30 AM
Ballroom E (Rhode Island Convention Center)
Shijia Wu, Jiangnan University, Wuxi, China
Nuo Duan, State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, China
Changqing Zhu, Inspection and Quarantine Bureau, Nanjing, China
Jingdong Shao, Jiangsu Entry-Exit Inspection and Quarantine Bureau of P.R.China, Nanjing, Jiangsu Province, China
Zhouping Wang, Jiangnan University, Wuxi, China
Introduction:   The Fumonisin B1 is a nephrotoxin in all species tested; a carcinogen and a reproductive toxicant in rodents, likely in humans. They are most frequently found in corn, corn-based foods and feeds, and other grains such as sorghum and rice. Rapid and effective measurement of Fumonisin B1 is of great importance for food safety.

Purpose:  We presented a new aptamer biosensor for Fumonisin B1, which was based on fluorescence resonance energy transfer (FRET) between upconversion fluorescent nanoparticles (UCNPs) and gold nanoparticles (Au NPs).

Methods:  The quencher (Au NPs) were attached to 5 end of the molecular beacons (MB) and the donor (UCNPs) attaching to 3 end of the MB. In the absence of target DNA (complementary DNA to FB1 aptamer), the energy donor and acceptor were taken into close proximity, leading to the quenching of fluorescence of UCNPs. Due to the combination between FB1 and FB1-specific aptamer, and caused the some complementary DNA dissociating from magnetic nanoparticles (MNPs). In the presence of the complementary DNA, the MB underwent spontaneous conformational change and caused the UCNPs and Au NPs to detach from each other, resulting in the restoration of UCNPs fluorescence.

Results:  The fluorescence of UCNPs was restored in a FB1 concentration-dependent manner, which built the foundation of FB1 quantification. The biosensor provided a linear range from 0.01 to 100 ng/ml for FB1 with a detection limit of 0.01 ng/ml in an aqueous buffer. As a practical application, the biosensor was used to monitor FB1 level in naturally contaminated maize samples with the results consistent with that of a classic ELISA method, indicating that the UCNPs-FRET biosensor was competent for directly sensing FB1in foodstuffs samples without optical interference, which benefited from the near infrared (NIR) excitation nature of UCNPs.

Significance:  This work opened the opportunity to develop biosensors for mycotoxins using the developed FRET system.