P1-222 Isolation and Identification (SPME-GC-MS) of Potential Spoilage Compounds Produced by Alicyclobacillus acidoterrestris in Orange and Apple Juices

Sunday, July 26, 2015
Exhibit Hall (Oregon Convention Center)
Leonardo Prado-Silva , University of Campinas , Campinas , Brazil
Adriana T. Godoy , Unicamp , Campinas , Brazil
Juan M. Oteiza , Centro de Investigación y Asistencia Técnica a la Industria Agroalimentaria , Neuquén , Argentina
Bernadette D. G. M. Franco , University of São Paulo , Sao Paulo , Brazil
Marcos N. Eberlin , University of Campinas , Campinas , Brazil
Anderson de Souza Sant'Ana , University of São Poalo , São Paolo , Brazil
Introduction: Alicyclobacillus acidoterrestris (AA) is cause of great concern for food industry due to its thermal and chemical resistances, as well as its spoilage potential. Despite this, not all AA strains are able to spoil fruit juices. In this way, identification of compounds produced by AA strains may assist on development of strategies to assess and control spoilage of fruit juices. 

Purpose: The objective of this study was to identify and quantify the production of guaiacol, and other potential compounds associated with AA spoilage in orange and apple juice (11ºBrix).

Methods: Initially, we evaluated 497 strains of A. acidoterrestris isolated from fruit juices and tomato-based products collected in Argentina and Brazil. The ability of the isolates to produce guaiacol was assessed through the use of an enzymatic method. Positive strains for guaiacol production were then individually inoculated at level of 102-3CFU ̸ ml in 10 ml of orange and apple juices, following storage at 45°C for 5 days. The techniques of micro-solid phase extraction by headspace (HS-SPME) and gas-chromatography with mass spectrometry (GC-MS) were used to identity and quantify volatile compounds produced by AA strains.

Results: From the 497 strains screened for guaiacol production, a total of 165 were confirmed by the enzymatic method to be able to produce guaiacol. Therefore, these strains were confirmed to be potentially deteriorigenic. CG-MS analysis was performed to further characterize and quantify the volatile compounds that can be associated with orange and apple juice spoilage by AA. A classification of AA strains in terms of their spoilage potential will be presented as well as the discrimination of volatile compounds produced by these strains.

Significance: This work will allow gaining insights on the incidence and spoilage potential of AA strains isolated from a variety of fruit-based products marketed in Argentina and Brazil.